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H. Irving Crane Papers,
1927-1950 (bulk 1935-1945) |
Extent and Forms of Material: 5.5 cubic feet, including photographs
and fabric samples (12 boxes)
Creator: H. Irving Crane
Abstract: H. Irving Crane worked as a chemist for Atlantic Research Associates, Inc.
(a division of National Dairy Corporation) from 1933-1940s on the production of several
products utilizing casein, a protein found in milk. These products include Aralac (a synthetic fiber),
Aracide (a fungicide and moth repellant), spray-dried milk, casein paints, and synthetic rubbers.
The H. Irving Crane papers document Crane's work as a chemist at Atlantic Research Associates, Inc.
and the development of Aralac and Aracide.
Repository: Archives Center, National Museum of American History,
Smithsonian Institution, Washington, D.C. archivescenter@si.edu
202-633-3270
www.americanhistory.si.edu/archives
Collection Number: AC1119
Processing Note: Processed by Elizabeth Garber (intern), June, 2009; supervised by Alison Oswald, archivist.
© 2009 by the Smithsonian Institution. All rights reserved.

Information for users of
the collection
Conditions Governing Access: The collection
is open for research use.
Conditions Governing Reproduction and Use: Copyright held by the Smithsonian Institution.
Collection items available for reproduction, but the Archives Center makes no guarantees concerning
copyright restrictions. Other intellectual property rights may apply. Reproduction permission from
Archives Center: reproduction fees may apply.
Preferred Citation: Title and date of item, H. Irving Crane Papers, 1927-1950,
Archives Center, National Museum of American History, Smithsonian Institution, box number X,
folder number XX, digital file number XXXXXXXX

In-depth information about the collection
- Administrative/biographical history
Scope and content
- System of arrangement
Acquisition information
Custodial History
Related artifacts
Access points
Container listing
-
Horace Irving Crane (1912-1984) was born on May 12, 1912.
In 1929, he enrolled at the Massachusetts Institute of Technology (MIT)
where he earned an undergraduate degree in Chemistry in 1933 and a Ph.D. in Chemistry in 1936.
In 1933, Crane began working at Atlantic Research Associates, Inc. (ARA) in Newtonville,
Massachusetts as a chemist. ARA was a division of National Dairy Products Corporation,
which was later absorbed by Kraft Foods. ARA specialized in the development of products
from casein, a protein found in milk. ARA had manufactured casein-based paints since 1927
and continued to produce other casein products such as glues, plastics, films, and paper coatings.
Most of these products were given a name beginning with the prefix "Ara-" taken from the company's name.
Crane and other chemists at ARA began research into the production of a casein fiber in 1937.
Aralac was first manufactured at a plant in Bristol, Rhode Island. Patents were granted to the
president of ARA, Francis Clarke Atwood, for Aralac ("Method of Making Proteinaceous Fibers"
US Patent #2,342,994 and "Method of Treating Fibrous Material and Product Resulting Therefrom"
US Patent #2,342,634). In 1941, production moved to a larger plant in Taftville, Connecticut.
The production of the fiber was as follows:
First the pH value of the milk was lowered using acid.
The protein reached its minimum solubility, and with swelling was
precipitated out of the milk as curd. This curd was the raw material
for the production of Aralac. The casein (curd) was collected in small
creameries as well as large ones. One hundred pounds of milk produced
3.7 pounds of casein, which in turn produced 3.7 pounds of fiber.
After the casein arrived at the plant, it was carefully blended with
casein from other producers and dissolved in water with proper solvents.
Adjustments were made to the viscosity in order to produce a uniform
base and ensure the complete removal of foreign materials. The solution
became syrup-like and was forced through a spinnerette into a coagulating
bath and was carried away. It remained in tow form through a succession of
hardening and molecular modifying treatments interspersed at times with washing and drying.
Aralac is in the Azlon class of fibers. Fibers in this class are made from regenerated,
naturally-occurring proteins such as milk, corn, soybeans, and peanuts. It was hoped that
Aralac would be considered a luxury fiber in direct competition with the best grades of wool.
It was introduced just as the United States entered World War II; during the war, Aralac was
blended with rayon and acetate for use in civilian dress fabric and in felted hats. It was
tested for use in carpet, military socks, lace, and knitting yarn, but was not satisfactory.
Due to its low strength and the difficulty in dyeing it, Aralac had a short life. Production of the fiber ended in 1948.
Crane also worked on Aracide, a moth and mildew repellant. Aracide was initially developed as a fungicide for casein
paints in 1937, but was also used to prevent moths from infesting Aralac. ARA attempted to obtain a patent for Aracide,
but was rejected due to similarities with another patented fungicide.
In addition to Aralac and Aracide, Crane worked on a spray drier to evaporate milk and other assorted ARA projects. In 1945,
ARA was reorganized and consolidated into a larger company, National Atlantic Research Corporation.
Following his departure from ARA, Crane worked at Sylvania Electric Products, Clevite Transistor, Computer Controls
Corporation, and Honeywell. In 1957, Crane received a patent for methods of treating Germanium in relation to
semiconductors (US Patent #2,793,146) while at Sylvania Electric Products.
Crane married his ARA lab technician, Laura Soule, and they raised their children in Massachusetts. He retired in 1977 and died in Vermont on April 7, 1984.
The H. Irving Crane papers illuminate the development of casein products in the 1930s-1940s,
particularly a fiber and fungicide. The collection is divided into two series:
Series 1, Atlantic Research Associates, Inc., 1927-1950,,
consists of material relating to Crane's research and experiments while a chemist at ARA.
This series is divided into eight subseries:
Subseries 1, Aralac, 1938-1945, illuminates the development, testing, production,
and uses of the casein fiber Aralac. Correspondence, memoranda, notes, and reports
document the challenges associated with the initial production, dyeing, and adding of
chemical washes to Aralac and the use of Aralac in manufacturing of cloth goods.
Correspondence between ARA and customers documents the use of Aralac in carpet, military
socks, lace, knitting yarn, and hats. Associated fiber samples from the dyeing process and
material relating to the treatment of Aralac with Aracide are also included.
Subseries 2, Aracide, 1935-1945, consists of correspondence, memoranda, notes, and reports
relating to the anti-fungal agent. Another ARA employee, Laura Adams, produced several reports on
Aracide. Correspondence reflects its testing for use in carpets and an attempt to obtain a patent for the fungicide.
Subseries 3, Other products, 1937-1945, contains materials relating to all the products that Crane worked on,
including a spray drying process for milk dehydration and casein paints. There is a small amount of documentation
of Aralac and Aracide within this subseries.
Subseries 4, Laboratory notebooks, 1937-1945, documents Crane's daily activities on the projects he worked on.
Arranged chronologically, test results, notes, graphs, and experimental procedures are recorded within these notebooks.
There are significant gaps in the date range listed above.
Subseries 5, Correspondence, memoranda, and reports, 1937-1948, records activities and communication within ARA.
Documents written by Crane relate to his work, but many other reports document projects that Crane was not directly
involved with. Two letters from F. C. Atwood, the president of ARA, illuminate occurrences within ARA:
the potential drafting of Crane into military service for World War II and the reorganization of the company into NARC.
Subseries 6, Reference materials, 1936-1948, is comprised of scientific resources that Crane utilized and created. He reviewed scientific literature, indexed and summarized
chemical abstracts, and compiled bibliographies related to the fields of fiber production, casein usage, and anti-fungal agents.
Subseries 7, Photographs, 1937-1941, illustrates ARA company gatherings, staff, and facilities.
Subseries 8, Printed material, 1927-1950, contains advertisements, catalogs, pamphlets, and brochures for assorted chemicals and laboratory equipment that were available to industrial chemists at the time. ARA-produced products represented include Aralac
and the paints Aratone, Aralux, and Casein Deep Colors. Additional periodicals and newsletters received by Crane are also included.
Series 2, Biographical Material, 1936-1947,,Biographical material, 1936-1947, documents Crane's educational background, insurance needs, banking, and time spent at work.
Fiber samples and oversize material have been separated from the collection for preservation concerns. Items separated are identified by folder.
- Series 1: Atlantic Research Associates, Inc., 1927-1950, undated
- Subseries 1, Aralac, 1938-1945, undated
- Subseries 2, Aracide, 1935-1945, undated
- Subseries 3, Other products, 1937-1945, undated
- Subseries 4, Laboratory notebooks, 1937-1945, undated
- Subseries 5, Correspondence, memoranda, and reports, 1937-1948, undated
- Subseries 6, Reference materials, 1936-1948, undated
- Subseries 7, Photographs, 1937-1941, undated
- Subseries 8, Printed materials, 1927-1950, undated
- Series 2: Biographical material, 1936-1947, undated
This collection was donated by H. Irving Crane's son, Andrew Crane, in October 2007.
Transferred to the Archives Center from the Division of Home and Community Life in October 2007.
The Division of Home and Community Life holds artifacts related
to this collection, including a suit made from Aralac (Accession
#2006.0096A).
Subject/Names:
Adams, Laura
Aracide
Araclone
Arafoam
Aralac
Aralux
Arapol
Aratone
Atlantic Research Associates, Inc.
Azlon fiber
Crane, H. Irving
National Atlantic Research Corporation
National Dairy Products Corporation
Magnavox
Subjects/Topical:
Casein
Chemical abstracts--Outlines, syllabi, etc.
Chemistry
Chemists
Fungicides
Fungicides--Testing
Spray drying
Synthetic fibers industry
Textile fibers, Synthetic
Textile fibers, Synthetic--Dyeing
Textile fibers, Synthetic--Equipment and supplies
Textile fibers, Synthetic--Laboratory manuals
Textile fibers, Synthetic--Testing
Wool, Artificial
Geographical:
Newtonville (Newton, Mass.)
Form/Genre:
Abstracts (summaries)
Advertisements--20th century
Cloth
Correspondence
Fiber
Graphs
Laboratory notebooks
Memoranda
Newsletters--20th century
Notebooks
Notes
Pamphlets
Periodicals
Photographs--20th century
Publications
Reports
Occupations:
Chemists
Scientists
| Box |
Folder |
|
| |
|
SERIES 1, ATLANTIC RESEARCH ASSOCIATES, INC., 1927-1950, UNDATED |
| |
|
Subseries 1, Aralac, 1938-1945, undated |
| 1 |
1 |
Casein, preparation, undated |
| |
2 |
Casein fiber – coagulation, hardening, 1938, undated |
| |
3 |
Casein fiber – softening treatments, 1938-1939, undated |
| |
4 |
Casein fiber – analytical methods, 1937-1943 |
| |
5 |
Ketenization of casein fiber, 1938, undated |
| |
6 |
Ketenization of casein fiber – mathematical treatment of results, 1938, undated |
| |
7 |
Aralac – Atlantic Research Associates [experimental?] spinning, 1939-1940, undated |
| |
8 |
Casein fiber – miscellaneous treatments, 1939-1945, undated |
| |
9 |
Casein fiber – dyeing, 1938-1942, undated |
| |
10 |
Dyes, dyeing, 1939-1942, undated |
| |
11 |
[Dye charts], 1941 |
| |
12 |
General Dyestuffs [Corporation], 1938-1942 |
| |
13 |
[Aratex, Inc. – Bristol, Rhode Island plant], 1940-1941, undated |
| |
14 |
Aralac – acid capacity and pH, 1939, undated |
| |
15 |
Aralac – customer contacts, 1940-1942 |
| |
16 |
[Assorted reports, memoranda, and notes], 1940-1941, undated |
| |
17 |
Strength tests – Atlantic Research Associates daily reports, 1940-1943 |
| |
18 |
[Newspaper clippings], 1938, 1942 |
| |
19 |
[Dyed fiber samples], undated |
| |
|
Subseries 2, Aracide, 1935-1945, undated |
| 2 |
1 |
[Memoranda, notes, and reports], 1935-1945, undated |
| |
2 |
Fungicides – Report by Miss [Laura] Adams, undated |
| |
3 |
Fungicides – Miss [Laura] Adams, 1938-1942, undated |
| |
4 |
Fungicides – miscellaneous notes, 1937-1940, undated |
| |
5 |
Alex Smith & Sons Carpet Company, 1939-1940 |
| |
6 |
[General], undated |
| |
7 |
[Reference materials], 1937-1940, undated |
| |
|
Subseries 3, Other products, 1937-1945, undated |
| |
8 |
[Assorted projects], 1944, undated |
| |
9 |
[Manual for preparation of casein paste paint], undated |
| |
10 |
[Water paints], undated |
| |
11 |
Gary plant reports, 1937 |
| |
12 |
[Lactic acid], 1942-1944, undated |
| 3 |
1 |
Acrylates [Arapol], 1942-1943, undated |
| |
2 |
Spray drier, 1944-1945, undated |
| |
3 |
Bobbitt Industrial Spec[ialties] Company, 1944-1945, undated |
| |
4 |
Corrosion, 1937, undated |
| |
5 |
[Tall oil soap and latex concentration], 1944-1945, undated |
| |
|
Subseries 4, Laboratory notebooks, 1937-1945, undated |
| |
6 |
[February – March 1937], 1937 |
| |
7 |
[February – June 1937], 1937 |
| |
8 |
1937 September 27 – 1937 December 31, 1937 |
| |
9 |
1938 September 30 – 1938 October 17, 1938 |
| |
10 |
1939 November 14 – 1940 April 4, 1939-1940 |
| 4 |
1 |
1941 August 18 – 1943 April 15, 1941-1943 |
| |
2-3 |
1943 October 14 – 1943 October 21, 1943-1944, undated |
| |
4-5 |
Work done on subjects other than Milk Dehydration, 1944-1945 |
| |
6 |
Casein fiber aftertreatments C-48 – C-94, 1938 |
| 5 |
1 |
Casein fiber aftertreatments C-95-, 1938 |
| |
2 |
[Procedural notebook], 1938, undated |
| |
|
Subseries 5, Correspondence, memoranda, and reports, 1937-1948, undated |
| |
3 |
Correspondence – H. I. Crane, 1937-1945 |
| |
4 |
[Correspondence regarding samples], 1946-1948 |
| |
5 |
[Atwood letters], 1942-1945 |
| |
6 |
[Boston Microchemical Society], 1946-1948 |
| |
7 |
[Weston Exposure Meter], 1945, undated |
| |
8 |
Crane – Memoranda, Reports, 1946 |
| |
9 |
Memoranda, 1940-1944 |
| |
10 |
Reports – H. I. Crane and others, 1939-1940 |
| |
11 |
Laboratory reports [by others], 1937-1939 |
| |
12 |
Weekly progress reports, 1938, undated |
| |
13 |
[Atlantic Research Associates Technical Bulletins], 1947-1948 |
| |
14 |
[Atlantic Research Associates envelopes], undated |
| |
| Subseries 6, Reference
material, 1936-1948, undated |
| |
15 |
[Testing procedures],
1941, undated |
| |
16 |
Aradization, 1940, undated |
| |
17 |
Abstracts, undated |
| |
18 |
[Abstracts], undated |
| |
19 |
[Abstracts], 1942, undated |
| 6 |
1 |
Chemical Abstracts, 1945-1948 |
| |
2 |
[Chemical Abstracts],
1946-1948 |
| |
3 |
Material for work report
– O. B. [Chemical Abstracts], 1947-1948 |
| |
4 |
Bibliographies, 1942-1946,
undated |
| |
5 |
[Articles, book excerpts,
and chemical abstracts], undated |
| |
6 |
[Notes], 1942, undated |
| |
7 | [Library Bulletin of
Abstracts Universal Oil Products], 1936-1938 |
| |
8 |
Books, 1939 |
| |
9 |
Casein and Its Industrial
Applications (book), 1939 |
| 7 |
1 |
[Literature Search
on Acrylates], 1940, undated |
| |
2 |
Ketene by catalysis,
undated |
| |
3 |
Lactates, Acetoxypropionates,
Acrylates, and related compounds, 1942 |
| |
4 |
Lanital, 1945-1947 |
| |
5 |
[Duties of an Atlantic
Research Associates lab assistant], undated |
| |
6 |
Subseries 7, Photographs,
1937-1941, undated |
| |
|
Subseries 8, Printed
material, 1927-1950, undated |
| |
7 |
[Atlantic Research
Associates product brochures], 1939-1944, undated |
| |
8 |
Leeds and Northrup,
1927-1937, undated |
| |
9 |
[Chemical advertisements
and information], 1933-1948, undated |
| |
10 |
[Chemical price lists],
1927-1947 |
| 8 |
1-2 |
[Laboratory equipment
advertisements and catalogs], 1933-1948, undated |
| |
3-4 |
[Newsletters and bulletins],
1930-1947, undated |
| |
5 |
[Milk], 1938, 1943 |
| |
6 |
[Consumer Reports],
1947 |
| |
7 |
[Chemistry –
history], 1928, 1933 |
| |
8 |
[Book advertisements],
undated |
| |
9 |
[Solicitations], 1944-1946 |
| |
10 |
Survival Under Atomic
Attack, 1950 |
| |
|
SERIES 2, BIOGRAPHICAL MATERIAL, 1936-1947, UNDATED |
| |
11 |
Massachusetts Institute
of Technology Qualification Record, 1936 |
| |
12 |
[Insurance, banking,
and other material], 1946-1947, undated |
| |
13 |
[Atlantic Research
Associates timesheets], 1944, undated |
| |
|
Material separated
for preservation reasons: |
| 9 |
1 |
Casein fiber –
dyeing, undated |
| |
2 |
Aratex, Inc. –
Bristol, Rhode Island plant, 1940, undated |
| |
3 |
Aratex, Inc. –
Bristol, Rhode Island plant and Aralac – customer contacts,
1941, undated |
| |
4 |
Crane – Memoranda,
reports, etc. and Reports – from H. I. Crane & others,
1940, undated |
| |
5-6 |
Reports – from
H. I. Crane and others, 1940-1941 |
| 10 |
1 |
Oversize papers, 1944 |
| |
2-4 |
Reports – from
H. I. Crane and others, 1941 and undated |
| |
5 |
[Dyed fiber samples],
undated |
| 11 |
1-4 |
[Dyed fiber samples],
undated |
| 12 |
1 |
[Loose fibers that
detached from dyed fiber samples], undated |
| |
2 |
[Aralac/rayon blend
fabric samples], undated |
| |
3-5 |
[Dyed fiber samples], undated |
|